The Vineyard Report

April candle winner: golfgod@torchlake.com
April, 2004 Vol 4, No. 4 

 

The Vineyard Farm

Vineyard Notes
Al Schneider - Old Friend Gone
Determining SO2
April Grape Recipe
From our readers
Candle W*nner & Laugh of the Month

The Candle - Honey Farm

New E-Commerce Site on line
April at the Honey Farm
Tests Fined Altered Honey
April Honey Recipe
From our readers
Candle W*nner & Laugh of the Month



Vineyard in April -
Pruning Season Begins

Vineyard in April. Pruning season has begun. The vines will not look like the picture on the left, they will all be given "haircuts." We have about 25 youths coming out this season during Easter break when they are off school.

Click here to see how we prune our vines.

 


Albert Schneider passed away late February at young age of 72.

He was very instrument in Pat & I becoming winemakers.

Shortly after Pat & I were married (more than 30 years ago) we decided to take a winemaking class at a local school at night. (Pat's class in something else got cancelled so she joined mine). It was a very interesting class. The instructor, Al Schneider, was very interested in what he was teaching. We continued to see him occasionally for the next 30 years. He grew grapes in his back yard a few miles South of us (in Oakland, Michigan) and made wine every year. He would visit us in the fall to fill his containers with honey from our Bulk Tank.

His wife, Helen called us a few weeks ago. We will miss him very much.

Try Al & Helen Schneiders recipe for "Chicken Salad with Grapes" or their "Harvest Salad," our April Grape Recipes below.

 


Sandy Paetz just sent me an update about what he is doing at the MSU Viticulture & Enology Program.

This program was brought to our attention a few years ago when a MSU student, Bernard Call, who is taking this course, purchased some grapes at our farm and was carefully measuring the brix of the grapes with a refractometer. The following year he returned to our farm after being in the program for one year and he was very enthusiastic, interesting and knowledgeable about the course.

Sandy Paetz, one of our past Sales Stand Associates, had also enrolled in the MSU program. When the two of them found out that they both were taking the courses, the conversations became very stimulating and they agreed to forward some of their program notes to us for our newsletter.

We have some inside stories of what Bernard and Sandy are doing at MSU.


TECHNIQUES FOR DETERMINING SULFUR DIOXIDE IN WINE:
THE ASPIRATION METHOD, THE RIPPER METHOD AND THE TITRETTOR METHOD. - W.C. PAETZ   OCTOBER 2, 2003

Abstract:

We employed three different methods to measure the sulfite content of different samples of wine.
The “Aspiration” method involved removing SO2 from the wine by aeration into a solution that oxidized into sulfuric acid. This acid was titrated and the SO2 calculated from the titre volume.
The “Ripper” method involved titrating the wine sample directly with an iodine solution.
The “Titrettor” method involved the use of a prepared reagent sealed in a vacuum ampoule. The result of this test gave the free SO2 in mg/L.

INTRODUCTION:

Sulfur is a preservative, an antioxidant as well as an antiseptic. These characteristics have distinguished this chemical as the silver bullet of wine makers for literally centuries. “Sulfur dioxide (so2) is typically added to the whole fruit or must at crushing. It is a chemical that has been added in various forms to wines since the ancient wine makers of Egypt and Rome learned of it’s ability to prevent wine spoilage.” (1.)
As enologists we will be called upon to discern the exact amount of various chemicals that can help protect our labor of love.
“Knowledge of the actual concentration of free sulfur dioxide and the ability to adjust concentrations to a desired level are of immense importance in fine wine production.” (2.)
The controlling governments’ sanction limited use of this substance in the final product. In the United States the maximum allowable content is 350 parts per million. (350 mg/L)
“Sulfur dioxide permits the storage of many types of wine today that would not exist without it’s protection. In particular, it permits extended barrel maturation and bottle ageing… The adjustment must be made within plus or minus 10 mg/ L.” (3.)

The emphasis on controlling sulfites would be incomplete if I did not mention the U.S. Government requirement. “Since January 9, 1987 wines containing more than 10 parts per million of sulfur dioxide must carry a label statement such as: “Contains Sulfites” (3.)

One can readily discern the value of being able to measure the free and total SO2 in a wine sample at any stage of production. This gives credibility and rationale to support our experiment.


Materials and Methods

Aspiration Method:
1.) 20 mill wine sample Pinot Grigio
2.) 10 mill phosphoric acid 25% solution
3.) 10 mills hydrogen peroxide
4.) 2-3 media drop color
5.) Aspirator with water vacuum 1 l / minute flow rate
6.) Round bottom flask with two peripheral openings plus open on the top with a stopper.
7.) Receiving vile
8.) Pipette
9.) Micro burette

Method:
Flow rate checked. Pipettes submerged into wine. Air moving through the sample pulling free SO2 into the impinger with hydrogen peroxide. 20 mills of wine sample placed into the lower ball beaker. 10 mills of phosphoric acid added to wine sample. Closed with a seal. Impinger add 10 mills of hydrogen peroxide into top flask. Add 2-3 drops of color solution indicator until green. Vacuum checked. Adjust h2o to one liter / minute of air pulled through system. Fifteen minutes. Titrate end point.

Ripper Method:
1.) Pipette 25 ml
2.) Conical flask
3.) Burette with stop cock
4.) Iodine reagent
5.) Safety bulb
6.) 1% starch indicator
7.) sulfuric acid 25% solution
8.) Miller Thurgau wine sample


Pipette the sample 25 ml into a clean conical flask. Add 1-% starch solution with bulb pipette 1 ml. Add 5-ml sulfuric acid. Stir mix.
Place under burette with stopcock drop iodine gradually until color stays after mixing for thirty seconds. Read amount of iodine to change color solution.

Titrettor Method:
1.) valve assembly
2.) ampoule
3.) Sample of wine
4.) Potassium lodate iodide with Phosphoric acid reagent
5.) Wine sample Traminette.

Place flexible end of the valve assembly over the titret ampoule. Fill beaker with wine. Snap the valve assembly at the score mark. Insert in sample and squeeze control bar to extract some wine sample. Wait thirty seconds then continue. Shake titrattor to mix watch for change from blue to clear sample. When end point is observed hold the ampoule in a vertical position and read the scale.
Results
Please refer to table in appendix for results.


Discussion
All of these methods are interesting but certainly one of them must be more accurate. Speed and convenience may not have any relevance here. This is not a measurement that is subject to estimation.



Conclusion
This knowledge is of particular value to anyone who desires to make acceptable wine. I really believe that it would have been useful to use the same wine for all of the methods to see if the results are consistent. If there were a correlation it would be fascinating to observe.
It is also important to note that the SO2 measurement alone means very little if there is a big variance in the pH of the wine samples. The knowledge of these variables together would allow you to make an accurate decision regarding how much SO2 should be added. We need to know how much is bound, how much is free and what the total is. The ability to rapidly and accurately test samples for these data would be of significant value to any enologist.

Appendix

Wine Sample Aspiration Ripper Titrettor
Muller Thurgau 40 46.08 60
Pinot Grigio 12 8.96 16
Traminette 19.2 25.6 42
Chardonnay 5.6 7.68 17

 


References:

1.) M.W. Baldy Ph.D., The University Wine Course, A Wine Appreciation Text and Self-Tutorial. The Wine Appreciation Guild. (1998)
2.) R.P.Vine, Wine Making From Grape to Market Place.Plenum Publishers (2002)
3.) R.Ribereau-Gayon, Handbook of Enology Volume I, The Microbiology of Wine and Vinifications. John Wiley & Sons Ltd. (2000)

 

April Grape Recipes - Chicken Salad & Harvest Salad

Chicken Salad
Cook chicken untill done, skin and bone, cut into small pieces. Let cool. Cook rice till done. Mix everything together, then use enough mayonnaise for mixing.
Helen Schneider, Oakland, Michigan
  • 1 chicken breast
  • 1 cup celery, diced
  • 1-20 oz.can pineapple chunks, drained
  • 2-11 oz. cans mandarin orange segments, drained
  • 2 cups seedless grapes, cut in half
  • 1 cup rice mayonnaise

Harvest Salad
12 cups leaf lettuce
1 lb green & 1 lb red grapes (seedless)
½ lb cooked medium shrimp, peeled and deveined
¼ cup sliced green onions
1 package (3 oz) Oriental Ramen noodles
¼ cup raisons
¼ cup golden raisons
¼ cup toasted walnuts or sunflower kernels
Salad dressing of you choice.
In a large bowl, combine lettuce, grapes and shrimp.
Break Ramen noodles into small pieces (save the seasoning packet for another use) add to salad with the chow mein noodles, raisons, onion, and walnuts.
Drizzle with dressing, toss to coat. yield = 16 servings

Al & Helen Schneider - Oakland

Do you have a great honey recipe - please send it to us and we will put it in our newsletter.

From our readers

This is a section for comments/questions/recipes from our readers. Please read the comments & feel free to put your 2 cents worth in.

Please send me your comments ......

Visit the Readers Comments page to view all the content of these messages. Here are samples of this months e-mails:  

Wants to develop a Honey Farm & Vineyard,  ••   Removing honey bees?  ••   Newspaper called FarmWorld,  ••   Honey from friend in the Philippines,  ••   Planting some grape vines this spring,  ••   Use some of your pictures?  ••   New Bee Club Formed,  ••   Want 20lb of beeswax,  ••   Working in the vineyard this spring

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Our list of previous candle w*nners.


 

Click below for something silly to end this newsletter with.

Classy McGassey Monkey Tune

See You Next Month!

 

Last Months Newsletter - Feb/March, 2004

The Vineyard Farm

Vineyard Notes
Local Meaderies & Winemaking Shops

Must Analysis
Feb/March grape recipe
From our readers
Candle W*nner & Laugh of the Month

The Candle - Honey Farm

Changes to our WebSite
March at the Honey Farm
Honey, Have You Considered Yoga?
March Honey Recipe
From our readers
Candle W*nner & Laugh of the Month

 

 

Honeyflow Farm
4939 Mill Rd.    PO Box 275
Dryden, Michigan 48428
(810) 796-2344 (Phone & Fax)


Comments or questions concerning Honeyflow Farm should be addressed to wcs@honeyflowfarmREMOVETHISBIT.com